AFM,STM,SPALEED

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SPM and related Instruments, Equipment and Examples

A Besocke type STM

designed for low temperature, using a liquid He Cryostat in UHV, at Colorado School of Mines. See GXSM community: Group of P. Sutter

View of our (at CSM) Low Temperature Besocke STM Head

LT Besocke STM Head LT STM in Cryo

STM Head, inset left: with sample and ramp, STM in cryostat, only inner shield is shown.

UHV STM and Prep. Chamber

UHV STM and Prep Chamber

UHV system in forground. Left: Preperation chamber, right: STM chamber. Behind: STM electronics and GXSM control software.

Electronic Setup used by GXSM

Here, at CSM, we were using the (old) PCI32 DSP card, the WRM-Piezodrive and a selfbuild "Besocke" Switchpanel and a dedicated selfbuild current amplifier (IVC and Bias Voltage Buffer).

Besocke Switch and Piezodrive

Electronic Setup

View of the wired up Piezodrive:

  • Top: PCI32 AD/DA connection panel
  • Middle: "WRM Piezo Drive"
  • Bottom: "Besocke Switch Panel"

The layout of the 19" frontpanels is available in LaTeX format in the CVS, see here Gxsm/Docs/HardwareDoc/.

IVC and Bias Buffer

IVC Box

The IVC and Bias Buffer is directly attached to the UHV Feedthrough.

Scanning Tunneling Microscopy and Surface Science using GXSM - some Examples:

The popular Silicon (111) surface in 7x7 reconstruction

Si (111)  7x7

Viewed by STM in constant current mode (approx. 1nA) in UHV, positive bias.

Data was taken using an early version of GXSM in Hannover, Group of M. Horn- von Hoegen

High Orientated Pyrolytic Graphite (HOPG)

HOPG

Scanned by STM in air using constant height mode monitoring the tunneling current:

  • Tip: cut PtIr wire
  • Currend: at average 1.3nA, modulation amplitude is about 100pA
  • Bias: 100mV
  • "Atom" spacing is 2.5 Angstroem
  • Scan size: 65Å × 65Å
Data taken at the CSM, Group of P. Sutter.

Some Silicon (100) impressions

Si100 Surface

Large scale STM image of the Si (100) surface, featuring a screw disslocation! The "scratch" on top left was the result of some "tip-improvments"...

  • Tip: etched tungston wire
  • Scan size: 1455Å × 910Å, original image size was (2989x1869 pixels)

Data taken at the CSM, Group of P. Sutter.

Detailed view, cropped from original image data set above (319Å × 214Å)

Si100 ScrewDissloc 2D view

All image processing by GXSM

Same image, rendered in 3D

Si100 ScrewDissloc 3D MesaGL view

All image processing and 3D rendering performed by GXSM, using GL (or MesaGL)

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